Title: Nondestructive, Noncontact Quantification of Carbon Fiber Alignment and Orientation By High-speed Microwave Ellipsometry
Authors: Nina P. Basta, Shridhar Yarlagadda, Dirk Heider, Edward J. Garboczi, Christian J. Long, and Nathan D. Orloff
DOI: 10.33599/nasampe/s.19.1371
Abstract: Novel short-fiber composites facilitate the manufacture of tailorable feedstock for small formed parts. In these composites, the alignment and orientation of the short fibers must be controlled to achieve the desired composite properties. While there are several processing variables that can be correlated to fiber alignment and orientation, there is a need for a fast, nondestructive, noncontact measurement technique to quantify local alignment and orientation in real time. Such a technique would enable real-time control of processing variables, resulting in higher quality composites. Here, we propose high-speed microwave ellipsometry as such a technique. To evaluate our approach, we measured five short-fiber composites samples made from a four-layer stack of carbon-fiber mats. These samples included one known control sample and four blind samples that were unknown at the time of testing. The four blind samples were known to be either a control, a sample with all layers rotated by 5°, a sample with a single unknown layer rotated by 5°, or a sample with a single unknown layer rotated by 15°. In this paper, we present our results demonstrating the effectiveness of this technique and discuss a path for real-time, large-scale imaging of fiber alignment and orientation.
References: [1] S. W. Yurgartis, “Measurement of small angle fiber misalignments in continuous fiber composites,” Compos. Sci. Technol., vol. 30, no. 4, pp. 279–293, Jan. 1987. [2] A. Anwer and H. E. Naguib, “Multi-functional flexible carbon fiber composites with controlled fiber alignment using additive manufacturing,” Addit. Manuf., vol. 22, pp. 360–367, Aug. 2018. [3] Z. Li, A. Haigh, C. Soutis, and A. Gibson, “Principles and Applications of Microwave Testing for Woven and Non-Woven Carbon Fibre-Reinforced Polymer Composites: a Topical Review,” Appl. Compos. Mater., vol. 25, no. 4, pp. 965–982, Aug. 2018. [4] “Review on quality assurance along the CFRP value chain – Non-destructive testing of fabrics, preforms and CFRP by HF radio wave techniques - ScienceDirect.” [Online]. Available: https://www.sciencedirect.com/science/article/pii/S1359836815001419. [Accessed: 01-Feb-2019]. [5] G. Bardl et al., “Automated detection of yarn orientation in 3D-draped carbon fiber fabrics and preforms from eddy current data,” Compos. Part B Eng., vol. 96, pp. 312–324, Jul. 2016. [6] F. Gambou, B. Bayard, and G. Noyel, “Characterization of material anisotropy using microwave ellipsometry,” Microw. Opt. Technol. Lett., vol. 53, no. 9, pp. 1996–1998, 2011. [7] F. Sagnard, F. Bentabet, and C. Vignat, “In situ measurements of the complex permittivity of materials using reflection ellipsometry in the microwave band: theory (part I),” IEEE Trans. Instrum. Meas., vol. 54, no. 3, pp. 1266–1273, Jun. 2005. [8] F. Sagnard, F. Bentabet, and C. Vignat, “In situ measurements of the complex permittivity of materials using reflection ellipsometry in the microwave band: experiments (Part II),” IEEE Trans. Instrum. Meas., vol. 54, no. 3, pp. 1274–1282, Jun. 2005.
Conference: SAMPE 2019 - Charlotte, NC
Publication Date: 2019/05/20
SKU: TP19--1371
Pages: 11
Price: FREE
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