Title: New Interfacial and Wicking Evaluation of Carbon Fiber (CF)/Epoxy Composites by CF Tow Capillary Glass Tube Method (TCGTM) with Tripe-CF Fragmentation Test
Authors: Joung-Man Park, Jong-Hyun Kim, K, Lawrence DeVries
DOI: 10.33599/nasampe/s.22.0685
Abstract: Using the new CF tow capillary glass tube method (TCGTM), this study investigated the wetting, wicking and interfacial properties for three type CFs reinforced epoxy composites combined with a triple-fiber fragmentation test. The CFs TCGTM was performed to evaluate the wettability and wicking of CF tow with epoxy resin by measuring the height of impregnated epoxy front in capillary tube using three different type CFs and fiber volume fractions more practically. After curing the specimens, the visual contact angle between CF and epoxy was measured using FE-SEM photos directly. Wetting and wicking were also evaluated by measuring the impregnated length of epoxy droplets on the CF tow, and compared with the result by CF TCGTM. From all of the relating tests, the 50C type CF exhibited better wetting and wicking than the 60E type CF and the desized CF. Interfacial shear strength (IFSS) were evaluated using a triple fiber fragmentation test for three different type CFs. Better IFSS of the 50C type CF was consistent with wetting and wicking results by CFs TCGTM. A new innovative CF TCGTM can be applicable for conventional CF reinforced epoxy composites more practically by combining with micromechanical test for the IFSS between single CF and epoxy mainly.
References: 1. Azlan MAM, Latif MRA, Abdullah MZ, Abidin KAZ, Wahab AA. Flow Behavior in the Resin Infusion of Glass Fiber Reinforced Polymer Wind Turbine Blade. Adv Mat Res 2013;686:118-24. 2. Jensen FM, Falzon BG, Ankersen J, Stang H. Structural testing and numerical simulation of a 34 m composite wind turbine blade. Compos Struct 2006;76:52-61. 3. Ganapathi AS, Joshi SC, Chen Z. Experimental and numerical investigation of process-induced deformations of glass/epoxy wind turbine blade spar cap. J Compos Mater 2017;51:3791-806. 4. Wang WX, Matsubara T, Hu J, Odahara S, Nagai T, Karasutani T, Ohya Y. Experimental investigation into the influence of the flanged diffuser on the dynamic behavior of CFRP blade of a shrouded wind turbine. Renewable Energy 2015;78:386-97. 5. Fagan EM, Flanagan M, Leen SB, Flanagan T, Doyle A, Goggins J. Physical experimental static testing and structural design optimisation for a composite wind turbine blade. Compos Struct 2017;164:90-103. 6. Langemeier P, Scheuer C. Big challenges: the role of resin in wind turbine rotor blade development. Reinf Plast 2010;l54:36-9. 7. Elia A, Taylor M, Gallachoir BO, Rogan F. Wind turbine cost reduction: A detailed bottom-up analysis of innovation drivers. Energy Policy 2020;147:111912. 8. Giorgi MD, Nobile R, Saponaro A. Numerical and experimental validation of SMArt thermography for the inspection of wind blade composite laminate. SN Appl Sci 2020; 2:1662. 9. Pradeep AV, Prasad SVS, Suryam LV, Kumari PP. A comprehensive review on contemporary materials used for blades of wind turbine. Mater Today Proc 2019;19:556- 10. Saba N, Paridah MT, Jawaid M. Mechanical properties of kenaf fibre reinforced polymer composite: a review. Constr Build Mater 2015;76:87-96. 11. Ma Q, Yang Z, Gu Y, Li M, Wang S, Zhang Z. Permeabilities along fiber direction of ramie bundles and through-thickness of ramie fabric stack for liquid composite molding. J Reinf Plast Compos 2017;36:40-52. 12. Salvatori D, Caglar B, Teixido H, Michaud V. Permeability and capillary effects in a channel-wise non-crimp fabric. Compos Part A 2018;108:41-52. 13. Vo HN, Pucci MF, Corn S, Moigne NL, Garat W, Drapier S, Liotier PJ. Capillary wicking in bio-based reinforcements undergoing swelling - Dual scale consideration of porous medium. Compos Part A 2020;134:105893. 14. Caglar B, Tekin C, Karasu F, Michaud V. Assessment of capillary phenomena in liquid composite molding. Compos Part A 2019;120:73-83. 15. Massodi R, Pillai KM. Darcy’s Law-Based Model for Wicking in Paper-Like Swelling Porous Media. Fluid Mech Transp Phenom 2010;56:2257-67. 16. Washburn EW. The dynamics of capillary flow. Phys Rev 1921;17:273-83. 17. Abida M, Gehring F, Mars J, Vivet A, Dammak F, Haddar M. Hygro-mechanical coupling and multiscale swelling coefficients assessment of flax yarns and flax/epoxy composites. Compos Part A 2020;136:105914. 18. Liu F, Shi Z, Dong Y. Improved wettability and interfacial adhesion in carbon fibre/epoxy composites via an aqueous epoxy sizing agent. Compos Part A 2018;112:337-45. 19. Wu Z, Cui H, Chen L, Jiang D, Wang L, Ma Y, Li X, Zhang X, Liu H, Wang N, Zhang J, Ma Y, Zhang M, Huang Y, Guo Z. Interfacially reinforced unsaturated polyester carbon fiber composites with a vinyl ester-carbon nanotubes sizing agent. Compos Sci Technol 2018;164:195-203. 20. Yao J, Fang Q, Zhang G, Yang C, Niu K. Effect of hydrophilic-hydrophobic ratio in self-emulsifying amphiphilic epoxy sizing agent on interfacial properties of carbon fibre/epoxy composites. Prog Org Coat 2020;143:105621. 21. Lu C, Wang J, Lu X, Zheng T, Liu Y, Wang X, Zhang D, Seveno D. Wettability and Interfacial Properties of Carbon Fiber and Poly(ether ether ketone) Fiber Hybrid Composite. ACS Appl Mater Interfaces 2019:11;31520-31. 22. Kim JH, Kwon DJ, Shin PS, Park HS, Baek YM, DeVries KL, Park JM. Evaluation of interfacial and mechanical properties of glass fiber and p-DCPD composites with surface treatment of glass fiber. Compos Part B 2018;153:420-8. 23. Shin PS, Kim JH, Park HS, Baek YM, Kwon DJ, DeVries KL, Park JM. Advanced interfacial properties of glass fiber/dopamine-epoxy composites using a microdroplet pull-out test and acoustic emission. J Adhes 2019:97;438-55. 24. Park JM, Kim JW, Goda K. A new method of evaluating the interfacial properties of composites. Compos Sci Technol 2000:60;439-50. 25. Park HS, Shin PS, Kim JH, Baek YM, Kwon DJ, Lee WI, DeVries KL, Park JM. Evaluation of Interfacial and Mechanical Properties of Glass. Fibers Polym 2018:19;1989-96. 26. Gagani AI, Krauklis AE, Sæter E, Vedvik NP, Echtermeyer AT. A novel method for testing and determining ILSS for marine and offshore composites. Compos Struct 2019:220;431-40. 27. Gaurav A, Singh KK. ILSS improvement of quasi-isotropic glass fiber reinforced epoxy laminate enhanced with arc discharged multi-walled carbon nanotube. Mater Today: Proc 2018:5;8638-44. 28. Drzal LT, Rich MJ, Lloyd PF. Adhesion of graphite fibers to epoxy matrices: I. The role of fiber surface treatment. J Adhes 1983;16:1-30.
Conference: SAMPE 2022
Publication Date: 2022/05/23
SKU: TP22-0000000685
Pages: 10
Price: $20.00
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