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Nano-Reinforced Potting Paste Compounds with Improved Mechanical Properties for Primary Structural Applications

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Title: Nano-Reinforced Potting Paste Compounds with Improved Mechanical Properties for Primary Structural Applications

Authors: Davood Askari, Amrith Pulipaka

DOI:

Abstract: Potting compounds play a critical role in aerospace sandwich composite structures, particularly for load transfer, void filling, sealing, and bonded insert applications. Enhancing their mechanical and adhesive performance without significant weight penalties remains a challenge. This study investigates the effects of multi-walled carbon nanotube (MWCNT) reinforcement on the compressive, adhesive, surface, and chemical properties of a commercial polyester-based potting compound. CNTs were incorporated at 0, 0.05, 0.10, 0.15, and 0.20 wt.% using a twostage dispersion process involving hand pre-mixing and three-roll milling. Mechanical performance was evaluated through compressive strength and single-lap shear testing, while surface wettability and chemical stability were assessed using water contact angle measurements and Fourier transform infrared spectroscopy (FTIR). Results demonstrate that low CNT concentrations (≤0.10 wt.%) considerably improve compressive strength and may negatively impact lap shear performance, while higher concentrations lead to increased brittleness and reduced strain-to-failure. FTIR analysis confirmed no chemical degradation of the polymer matrix and contact angle measurements indicated persistent hydrophilic behavior. These findings highlight the importance of optimized CNT content and dispersion for aerospace-grade potting compounds for primary structural applications.

References: 1. I. Baylakoglu, C. Hillman, and M. Pecht, “Characterization of some commercial thermally-cured potting materials,” in International IEEE Conference on the Business of Electronic Product Reliability and Liability, Hong Kong, January, pp. 15–17, 2003. 2. K. D. PATE, “Chapter 25 - applications of adhesives in aerospace,” in Adhesion Science and Engineering (D. Dillard, A. Pocius, and M. Chaudhury, eds.), pp. 1129–1192, Amsterdam: Elsevier Science B.V., 2002. 3. EpoxySet Inc, “Types of Potting Compounds: Epoxy, Urethane & Silicone Explained,” Apr. 2015. https://epoxysetinc.com/uncategorized/different-types-of-potting-compounds. [Accessed 24th July 2025]. 4. C. Corporation, “Potting materials | Encapsulants & Underfills | CAPLINQ Corporation.” http://www.caplinq.com/potting-materials.html. [Accessed 25th July 2025]. 5. S. Schauer, “Aircraft Assembly: Great Potential for Automation,” Dec. 2019. https://www.viscotec.de/en/aircraft-assembly-great-potential-for-automation/ [Ac-cessed: 5th December 2025]. 6. CompositesWorld, “Lightweight Potting Compounds Provide Enhanced Mechanical Strength,” Sept. 2025. https://www.compositesworld.com/articles/lightweight-pottingcompound-provides-enhanced-mechanical-strength. [Accessed: 24th September 2025]. 7. “Marine Applications for Adhesives and Sealants | Adhesives & Sealants Industry.” https://www.adhesivesmag.com/articles/97993-marine-applications-for-adhesives-andsealants [Accessed: 29th September 2025]. 8. “Epoxies Offer Innovative Solutions for the Wind Power Industry | Master-Bond.com.” https://www.masterbond.com/articles/epoxies-offer-innovative-solutions-wind-powerindustry [Accessed: 2nd October 2025]. 9. “Wind Blades: Progress and Challenges,” Dec. 2025, https://www.compositesworld.com/ articles/wind-blades-progress-and-challenges, [Accessed: 5th December 2025]. 10. “NAS Standard Potted Inserts | Clarendon Made.” https://www.clarendonsf.com/products /inserts/potted-inserts [Accessed: 5th December 2025]. 11. MTS, “MTS.” https://www.mts.com/en/products/materials/static-materials-testsystems/criterion-electromechanical [Accessed: 5th December 2025]. 12. J. Stefinsky, “Digital Rockwell Hardness Tester,” 13. MTS, “Water Contact.” https://www.ossila.com/cdn/shop/files/contact-angle-featuredimage.jpg?v=1754399698 [Accessed: 5th December 2025]. 14. M. Singh, S. Palaniappan, S. M R, and S. Siengchin, “Emerging trends in nanofiller composites for aerospace and automobile performance enhancement,” Journal of Engineering and Applied Sciences, vol. 12, p. 7, Jan. 2025. 15. F.-Z. Zhang, X.-B. Liu, C.-M. Yang, G.-D. Chen, Y. Meng, H.-B. Zhou, and S.-H. Zhang, “Insights into robust carbon nanotubes in tribology: From nano to macro,” Materials Today, vol. 74, pp. 203–234, May 2024. 16. A. Mokhalingam and S. S. Gupta, “Helical single-walled carbon nanotubes under mechanical and electrostatic loading,” Carbon Trends, vol. 9, p. 100204, Oct. 2022. 17. B. Ribeiro, E. C. Botelho, M. L. Costa, and C. F. Bandeira, “Carbon nanotube buckypaper reinforced polymer composites: a review,” Polímeros, vol. 27, pp. 247–255, Sept. 2017. 18. S. Singh, S. Vardharajula, P. Tiwari, Erdal Eroğlu, Komal Vig, V. Dennis, and Ali, “Functionalized carbon nanotubes: biomedical applications,” International Journal of Nanomedicine, p. 5361, Oct. 2012. 19. R. Gulotty, M. Castellino, P. Jagdale, A. Tagliaferro, and A. A. Balandin, “Effects of Functionalization on Thermal Properties of Single-Wall and Multi-Wall Carbon Nanotube–Polymer Nanocomposites,” ACS Nano, vol. 7, pp. 5114–5121, June 2013. 20. M. Ardjmand, M. Omidi, and M. Choolaei, “The effects of functionalized multi-walled carbon nanotube on mechanical properties of multi-walled carbon nanotube/epoxy composites,” Oriental Journal of Chemistry, vol. 31, pp. 2291–2301, Dec. 2015. 21. W. Yulistia and M.., “The Effect of Graphitization Temperature on the Composition and the Electrical Conductivity of Carbon Nanotube,” KnE Engineering, vol. 1, p. 323, Apr. 2019. 22. R. Vijayan, A. Ghazinezami, S.R. Taklimi, M.Y. Khan, D. Askari, The geometrical advantages of helical carbon nanotubes for high-performance multifunctional polymeric nanocomposites, Composites Part B: Engineering, 156 (2019) 28–42. 23. R. Sritharan, D. Askari, Enhancing the short-beam strength of composite laminates using helical carbon nanotubes, Composites Part B: Engineering, 221 (2021) 108999. 24. R. Sritharan, D. Askari, Improvement of the tensile properties of laminated composites reinforced with Heli‐Coil forms of carbon nanotubes, Polymer Composites, 44(10) (2023) 7070–7083. 25. D. Askari, S.R. Taklimi, A. Ghazinezami, Helical carbon nanotubes, US Patent Application 16/421,049, 2019 26. D. Askari, Nanocomposites with interlocking nanostructures, U.S. Patent Application 16/146,839. 27. R. Sritharan, S.R. Taklimi, A. Ghazinezami, D. Askari, The chemical functionalization advantages of carbon nano heli-coil reinforcements for multifunctional polymeric nanocomposites, Journal of Composite Materials, 59(14) (2025) 1705–1720.

Conference: SAMPE 2026

Publication Date: 2026/04/27

SKU: 72

Pages: 18

Price: $36.00

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